Author(s): Maryam Ashour, Farouk Kandil, Abdulkader Alazrak

Email(s): maryam1.ashour@damascusuniversity.edu.sy , farouk , kandil1@damascusuniversity.edu.sy , abdulkader.alazrak@damascusuniversity.edu.sy.

DOI: 10.52711/0974-360X.2024.00235   

Address: Maryam Ashour1, Farouk Kandil2, Abdulkader Alazrak2
1Ph. D., Student, Department of Chemistry, Faculty of Science, Damascus University, Syria.
2Ph. D., Department of Chemistry, Faculty of Science, Damascus University, Syria.
*Corresponding Author

Published In:   Volume - 17,      Issue - 4,     Year - 2024


ABSTRACT:
Some of triazole derivatives were synthesized by cyclization reaction, of thiocarbohydrazide was synthesized by reaction of carbon disulfide and aqueous hydrazine, the basic nucleus 4-amino- 3- methyl -1, 2, 4-triazole-5-thione(L) was prepared by reaction of thiocarbohydrazide compound with glacial acetic acid under reflux condition.The compound(L) was subjected to addition reaction with different aldehydes to synthesize Schiff bases N,N bis(3-methyl-1,2,4-triazole-5- thione (1,3-methylidene )benzene (L1) and N, N bis(3-methyl-1,2,4-triazole-5- thione (1,4- methylidene )benzene (L2). The compound (L1),(L2) were confirmed by their melting point,FTIR,U.V-visible ,1HNMR spectra


Cite this article:
Maryam Ashour, Farouk Kandil, Abdulkader Alazrak. Synthesis, and Spectroscopic Characterization study of some Schiff Bases N, N bis (3-methyl-1,2,4-triazole-5- thione (1,3-methylidene) benzene and N, N bis (3-methyl-1,2,4-triazole-5- thione (1,4- methylidene) benzene. Research Journal of Pharmacy and Technology.2024; 17(4):1486-0. doi: 10.52711/0974-360X.2024.00235

Cite(Electronic):
Maryam Ashour, Farouk Kandil, Abdulkader Alazrak. Synthesis, and Spectroscopic Characterization study of some Schiff Bases N, N bis (3-methyl-1,2,4-triazole-5- thione (1,3-methylidene) benzene and N, N bis (3-methyl-1,2,4-triazole-5- thione (1,4- methylidene) benzene. Research Journal of Pharmacy and Technology.2024; 17(4):1486-0. doi: 10.52711/0974-360X.2024.00235   Available on: https://rjptonline.org/AbstractView.aspx?PID=2024-17-4-9


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